Method The column was packed with ODS, using ethyl parahydroxybenzoate as internal standard. The mobile phase was a mixture of 0.2% ammonium carbonate-acetonitrile-tetrahydrofuran ( 42 ∶ 39 ∶ 19). Chromatography was performed with ultraviolet detector at 238 nm. 方法以ODS为固定相,羟苯甲酸乙酯为内标物,以0.2%碳酸铵溶液-乙腈-四氢呋喃(42∶39∶19)为流动相,检测波长为238nm,流速1.0mL·min-1。